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Beilstein J. Org. Chem. 2018, 14, 515–522, doi:10.3762/bjoc.14.37
Graphical Abstract
Scheme 1: Previously reported procedure for the addition of ketene dithioacetals to α,β-unsaturated ketones [33] ...
Scheme 2: Addition of dithi(ol)anylium TFBs to α,β-unsaturated non-cyclic ketones.
Scheme 3: Addition of dithi(ol)anylium TFBs to α,β-unsaturated cyclic ketones.
Scheme 4: Single versus double addition of ketones to dithiolanylium TFB 1e. adr was calculated from the 1H N...
Scheme 5: The scope of the presented protocol demonstrated by examples including the use of additional electr...
Scheme 6: Synthesis of diene dithioacetals 18a and 18b by addition of ynone 17 to α-alkyl or aryl-substitued ...
Beilstein J. Org. Chem. 2012, 8, 1191–1199, doi:10.3762/bjoc.8.132
Scheme 1: Diverse synthesis of indoles using Bartoli reactions. aSee [24].
Figure 1: Nitroarenes on solid supports. In red: Nitroarenes failed to give indoles. aResin has been reported...
Figure 2: Temperature optimization with Grignard reagent 2{b}.
Figure 3: Temperature optimization with Grignard reagent 2{a}. Isolated yield.
Figure 4: Optimization studies of ester 1{h} with a Grignard reagent 2{d} to give indole 3{h,d} and methyl 3-...
Scheme 2: Stille reaction on solid supports.
Scheme 3: Suzuki reaction on solid supports.
Scheme 4: Sonogashira–Hagihara reaction on solid supports.